On Sulphonfluoresceïn and Some of Its Derivatives

by C. W. Hayes

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ON
SULPHONFLUORESCEÏN
AND SOME OF ITS DERIVATIVES.

DISSERTATION

Presented for the Degree
of
Doctor of Philosophy
at the
Johns Hopkins University

by
C. Willard Hayes,
1887.

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		p.
	Introduction	[ 3.]
I	Ortho-sulpho-benzoic acid.
	Preparation from toluene and H2SO4	[ 7.]
	”   ” para-nitro-toluene and H2SO4	[ 8.]
	Oxidation  of  toluene - o - sodium sulphonate	[12.]
	Preparation of Sulphinide from ”   ”	[14.]
	”   ”   ”  by chlorsulphonic acid.	[17.]
	Conversion of sulphinide into o-sulphobenzoic acid.	[25.]
	Analysis of and crystallography of  ”  ”   ”	[28.]
II	Sulphonfluoresceïn—previous attempts	[29.]
	Preparation and purification of s-fluoresceïn	[30.]
	Analyses of          ”	[34.]
	Properties of          ”	[35.]
	Salts. Ba. and Ca. of       ”	[37.]
	Acetyl derivative of        ”	[41.]
	Br substitution products of    ”	[42.]
	Action of H2SO4 on       ”	[44.]
	Action of HCl on         ”	[45.]
	Reduction of          ”	[46.]
	Conclusion.	[47.]

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On Sulphonfluoresceïn and some of its Derivatives.