Separating Calorimeter—The separating calorimeter mechanically separates the entrained water from the steam and collects it in a reservoir, where its amount is [Pg 133] either indicated by a gauge glass or is drained off and weighed. Fig. 17 shows a calorimeter of this type. The steam passes out of the calorimeter through an orifice of known size so that its total amount can be calculated or it can be weighed. A gauge is ordinarily provided with this type of calorimeter, which shows the pressure in its inner chamber and the flow of steam for a given period, this latter scale being graduated by trial.
Fig. 17. Separating Calorimeter
The instrument, like a throttling calorimeter, should be well insulated to prevent losses from radiation.
While theoretically the separating calorimeter is not limited in capacity, it is well in cases where the percentage of moisture present in the steam is known to be high, to attach a throttling calorimeter to its exhaust. This, in effect, is the using of the separating calorimeter as a small separator between the sampling nozzle and the throttling instrument, and is necessary to insure the determination of the full percentage of moisture in the steam. The sum of the percentages shown by the two instruments is the moisture content of the steam.
The steam passing through a separating calorimeter may be calculated by Napier’s formula, the size of the orifice being known. There are objections to such a calculation, however, in that it is difficult to accurately determine the areas of such small orifices. Further, small orifices have a tendency to become partly closed by sediment that may be carried by the steam. The more accurate method of determining the amount of steam passing through the instrument is as follows:
A hose should be attached to the separator outlet leading to a vessel of water on a platform scale graduated to 1⁄100 of a pound. The steam outlet should be connected to another vessel of water resting on a second scale. In each case, the weight of each vessel and its contents should be noted. When ready for an observation, the instrument should be blown out thoroughly so that there will be no water within the separator. The separator drip should then be closed and the steam hose inserted into the vessel of water at the same instant. When the separator has accumulated a sufficient quantity of water, the valve of the instrument should be closed and the hose removed from the vessel of water. The separator should be emptied into the vessel on its scale. The final weight of each vessel and its contents are to be noted and the differences between the final and original weights will represent the weight of moisture collected by the separator and the weight of steam from which the moisture has been taken. The proportion of moisture can then be calculated from the following formula:
| x | = |
| (7) |
| Where [Pg 134] | x | = | per cent moisture in steam, |
| W | = | weight of steam condensed, | |
| w | = | weight of moisture as taken out by the separatingcalorimeter. | |
Sampling Nipple—The principle source of error in steam calorimeter determinations is the failure to obtain an average sample of the steam delivered by the boiler and it is extremely doubtful whether such a sample is ever obtained. The two governing features in the obtaining of such a sample are the type of sampling nozzle used and its location.