A lithium-drifted germanium-crystal gamma-ray detector. The large container is a reservoir of liquid nitrogen that keeps the detector cooled to a temperature of -196° Centigrade (321° below zero, Fahrenheit). The lead brick shield keeps out most of the gamma rays that come from naturally radioactive materials in the room. The plastic slots hold cards upon which the samples are mounted for counting. Sometimes the detector is arranged vertically and samples are placed on shelves above it.
What about the neutrons for the irradiation? Although there isn’t a suitable nuclear reactor[9] in your city, there is one at a university only an hour away by jet. Since it may take a few hours to get the sample to the counter after irradiation, you won’t be able to look for short-lived activation products, i.e., those with half-lives of up to an hour. However, this will exclude only a few elements from detection.
A pulse-height analyzer used for gamma-ray spectrometry. A gamma-ray spectrum is displayed on the television screen. Data is printed out automatically on the electric typewriter and also may be plotted as a graph on the paper to the left. In other systems, data may be coded onto punched paper tape as well. Such tape may be “read” by a computer that can be programmed to use the data to calculate what radioactive isotopes are present and their quantities.
Now you are ready to begin the analysis. This will be a qualitative analysis since you are merely looking for a significantly different element in that silicon crystal. How much of it is present is only of secondary interest. Therefore, if you find anything different, you will rely on an approximate calculation to tell you “how much”.
This is called a “swimming pool” reactor because the nuclear fuel, built into metal rods, is held in a framework at the bottom of a deep pool of water. The water serves as a shield to protect workers from the radiation and also helps the reactor “go” by slowing down neutrons to make them more likely to interact with the target atoms. “Swimming pool” reactors are frequently used for neutron activation analysis and typically provide neutron fluxes of over 10¹³ (10 million million) neutrons per square centimeter per second.
