Alum is also made from crude pyrites and other aluminous mixtures. It is first roasted in an enclosed area; then, after being exposed for some months to the air in order to soften it, it is thrown into vats and dissolved. After this the solution is poured into the leaden rectangular pans and boiled until it condenses into alum. The pyrites and other stones which are not mixed with alum alone, but which also contain vitriol, as is most usually the case, are both treated in the manner which I have already described. Finally, if metal is contained in the pyrites and other rock, this material must be dried, and from it either gold, silver, or copper is made in a furnace.
Vitriol[11] can be made by four different methods; by two of these methods from water containing vitriol; by one method from a solution of melanteria, sory and chalcitis; and by another method from earth or stones mixed with vitriol.
By the third method vitriol is made out of melanteria and sory. If the mines give an abundant supply of melanteria and sory, it is better to reject the chalcitis, and especially the misy, for from these the vitriol is impure, particularly from the misy. These materials having been dug and thrown into the tanks, they are first dissolved with water; then, in order to recover the pyrites from which copper is not rarely smelted and which forms a sediment at the bottom of the tanks, the solution is transferred to other vats, which are nine feet wide and three feet deep. Twigs and wood which float on the surface are lifted out with a broom made of twigs, and afterward all the sediment settles at the bottom of this vat. The solution is poured into a rectangular leaden caldron eight feet long, three feet wide, and the same in depth. In this caldron it is boiled until it becomes thick and viscous, when it is poured into a launder, through which it runs into another leaden caldron of the same size as the one described before.