In addition to these gas analyses, there are also made in the main laboratory, analyses and calorific tests of all coal samples collected by the Geological Survey in connection with its land-classification work on the coal lands of the Western States. Routine analyses of mine, car, and furnace samples of fuels for testing, before and after washing and briquetting, before coking and the resultant coke, and extraction analyses of binders for briquettes, etc., are also made in this laboratory.
The fuel-testing laboratory at Washington is equipped with three Mahler bomb calorimeters and the necessary balances and chemical equipment required in the proximate analysis of coal. More than 650 deliveries of coal are sampled each month for tests, representing 50,000 tons purchased per month, besides daily deliveries, on ship-board, of 550,000 tons of coal for the Panama Railroad. The data obtained by these tests furnish the basis for payment. The tests cover deliveries of coal to the forty odd bureaus, and to the District Municipal buildings in Washington; to the arsenals at Watertown, Mass., Frankford, Pa., and Rock Island, Ill.; and to a number of navy yards, through the Bureau of Yards and Docks; to military posts in various parts of the country; for the Quartermaster-General’s Department; to the Reclamation Service; to Indian Agencies and Soldiers’ Homes; to several lighthouse districts; and to the superintendents of the various public buildings throughout the United States, through the Treasury Department; etc. During 1909, the average rate of reporting fuel samples was 540 per month, requiring, on an average, six determinations per sample, or about 3,240 determinations per month.
Fuel-Research Laboratories.—Smaller laboratories, occupying, on the average, three rooms each, are located in Building No. 21. One is used for chemical investigations and calorific tests of petroleum collected from the various oil fields of the United States; another is used
for investigations relative to the extraction of coal and the rapidity of oxidization of coals by standard solutions of oxidizing agents; and another is occupied with investigations into the destructive distillation of coal. The researches under way show the wide variation in chemical composition and calorific value of the various crude oils, indicate the possibility of the extraction of coal constituents by solvents, and point to important results relative to the equilibrium of gases at high temperatures in furnaces and gas producers. The investigations also bear directly on the coking processes, especially the by-product process, as showing the varying proportion of each of the volatile products derivable from types of coals occurring in the various coal fields of the United States, the time and temperature at which these distillates are given off, the variation in quality and quantity of the products, according to the conditions of temperature, and, in addition, explain the deterioration of coals in storage, etc.
At the Washington office, microscopic investigations into the life history of coal, lignite, and peat are being conducted. These investigations have already progressed far enough to admit of the identification of some of the botanical constituents of the older peats and the younger lignites, and it is believed that the origin of the older lignites, and even of some of the more recent bituminous coals, may be developed through this examination.
In the chemical laboratories, in Building No. 21, the hoods (Figs. [11] and [12]) are of iron, with a brick pan underneath. They are supported on iron pipes, as are most of the other fixtures in the laboratories
in this building. The hood proper is of japanned, pressed-iron plate, No. 22 gauge, the same material being used for the boxes, slides, and bottom surrounding the hood. The sash is hung on red copper pulleys, and the corners of the hood are reinforced with pressed, japanned, riveted plate to which the ventilating pipe is riveted.