The Operation.
I pour’d a Drachm of Mercury twice distilled into a Glass Urinal, which I fill’d with Rain Water: Then I set the Vessel upon the naked Fire: The Water boil’d strongly for eight Hours, yet so that there still was some Water swimming over the Mercury. The Mercury being afterwards weigh’d, gave a Drachm without any Loss.
Again; I pour’d a Drachm of Mercury into a clean dry Glass Vessel. This I so fitted in a Kettle, that it cou’d not fall aside. I filled the Kettle with Water; I made the Water boil eight Hours. This Vessel was cylindrical, open, two Inches and one half deep, and placed so that the Water cou’d not get in. After this was so done, the Mercury weighed one Drachm without any Loss.
I put pure Mercury into a Glass Vessel, I poured Water upon it; and setting the Still over it, I boil’d it for a long while: No Mercury ascended. I continued boiling, till all the Water being gone out, the Mercury remained dry in the Bottom of the Vessel. However, I did not then increase the Fire; but the Mercury presently ascended to the Sides of the Vessel, and into the Head. The Reason of this appears from what I have written in my chemical Institutions about Water and Fire.
Experiment XIV.
Mercury may be chang’d by Art so as that it shall ascend from the Bottom of the Vessel, by the Heat of Vinegar, before it boils up.
The Operation.
Having made a Mass of a Pound and a half of Mercury, with half a Pound of Lead (the Chemists call such a Mass an Amalgama) I shook it in a Glass Vessel. There was produced a very black Powder. This I put into a Glass Cucurbite 14 Inches high; I pour’d pure distill’d Wine-Vinegar over it. By a gentle Distillation I took away the Phlegm. I then increased the Heat a little, but so that the Liquor did not boil. The Mercury ascended into the Head, together with the Phlegm, and thence into the Receiver. The same I tried and experienced other Ways. It is a Circumstance worthy a Chemist’s Speculation; but I shall say no more of it here. By much the like Artifice, I have seen Quicksilver made so volatile, that it was rais’d in my Digestory-Furnace with a less Degree of Heat, than that of a Man in Health, and ascended to the Sides of the Vessel. Do you think the Mercury was then purer? It was mix’d with Metal, and very dry. But perhaps I may some other time relate some very laborious Experiments which I have made for several Years, in examining Mercury and Metals, if I find that such Things are likely to meet with the Approbation of the Learned.