It was in August, 1894, that Selous went north for his first experiences of Highland sport. His destination was the Island of Mull, where for a fortnight he enjoyed the chase of the seal, the otter, and the wild goat, on the estate of Loch Buie, at the invitation of the Maclaine of Lochbuie. He thus describes his first search for seals and otters:—

"On August 16th, 1894, accompanied by the keepers MacColl and Nottman, I visited Loch Spelve in search of seals and otters. Skirting the shores of the loch in a small boat, we soon espied two seals lying out on a rock. They, however, winded us and slipped into the water, when we were still a long way off. We then went ashore and put the three terriers into a cairn which the keepers knew otters to be partial to, and from the behaviour of the dogs we soon became aware that one of the animals was somewhere about. Knowing that if the dogs succeeded in drawing the otter from the rocks it would make for the sea, I took up my position amongst the slippery seaweed covered with stones near the water and waited full of expectation. However, the otter resisted all the overtures of the terriers and would not bolt. Then MacColl, the wily, produced some evil-smelling fuse and, setting light to it, pushed it into a hole amongst the stones. The effect was magical, for the otter bolted at once almost between MacColl's legs. Instead, however, of coming towards the sea, it made back through the wood and took refuge in another cairn. From the second place of refuge another piece of fuse soon dislodged it, and this time making for the sea, it came past me in the open, travelling over the seaweed-covered rocks at no great pace. My first barrel knocked it over, but it quickly recovered itself, only to be again knocked down by my second left-hand barrel. This time it lay dead, and proved to be a fine bitch otter in excellent coat, weighing 14½ lbs. and measuring 3 ft. 6 ins. in length."

In January, 1895, he again went to Loch Buie and shot his first woodcock and other Highland game, and in January, 1897, he got his first pair of ptarmigan. It was in Ben Alder Forest that he killed his first Highland stags, but the chase of red deer as conducted in Scotland did not, as we should expect, greatly appeal to him.

In September, 1894, Selous and his wife reached Bournabat near Smyrna, where he remained a short time as the guest of H. O. Whittall. From here, accompanied by his wife and the Whittalls, Selous made a short trip into the interior, with the intention of finding haunts of the wild goat (Capra aegagrus). After an interesting journey amongst the Turks and Yuruks he returned to the sea-coast, where in the Musa Dagh he did some hunting, but was unsuccessful in finding the old billies, only killing one male with small horns. On October 3rd he returned to Smyrna, and then went straight into the Ak Dagh to look for the long-faced red deer. These animals are now scarce and difficult to hunt in the dense forests, and he only succeeded in coming up to one good fourteen-pointer, which he killed with a long shot on October 19th.

He was, however, somewhat fascinated with this hunting in Asia Minor, for though the game was comparatively scarce and hunting difficult, owing to the rough nature of the ground and abundance of local hunters, yet it satisfied his idea of what is called "high-class sport." Selous never liked to admit failure with any animal, so at the end of January, 1895, he again made a trip to Asia Minor in the hope of getting good specimens of the wild goat and, if possible, the black mouflon (Ovis gmelini). This time he decided to hunt the Maimun Dagh, a great mass of mountains situated close to the Smyrna railway. For a fortnight he toiled up and down its steep and parched cliffs, and then at last he saw and got a shot at one of the patriarchs with long horns. This goat he wounded very badly and lost, but some days later a Turk saw a large goat fall from a cliff and remain suspended by its horns in a tree, where he despatched it. This was without doubt the fine male which Selous had lost, and he was lucky enough to obtain the head. A few days later he found another grand billy, alas with only one horn. This he also killed and lost, but found it the next day. Two other fair specimens made up his bag, so on the whole the expedition was quite successful. Then he returned to England in February.

Although so recently married, Selous found that living in England was too expensive, and this, combined with the "call of the wild," which never left him, evolved a new spirit of restlessness and desire once more to live in the open veldt and to see the game. To this was added the request of an old friend, Mr. Maurice Heany, who asked him to go into Matabeleland and assist him in the management of a land and gold-mining company. After consulting his wife, who was willing to share the troubles and difficulties of the new country, Selous accepted the post, which was to occupy him for two years.

Accordingly Selous and his wife left England in March, 1895, and after spending two months in Cape Colony and the Free State, where he shot some springbuck, blesbuck, and black wildebeest for his collection, he took ship to Beira and then went by rail to Chimoio, where he met his waggon and oxen, and passed on via Salisbury, the Hanyane river, to Bulawayo. At the Sebakwe river he fired at what he thought was a jackal, but on arriving near the animal, which he expected to find dead, as he had heard the bullet strike, he was suddenly charged by a leopard. The angry beast passed right under his stirrup-iron, and after going thirty yards stopped and sat on its haunches. Another shot at once killed it.

The Selous now left for Essexvale, the farm of his company, and took up their quarters in a rough wood and mud two-roomed house which was to be their home until the wire-wove bungalow, which had been sent out from England in sections, should arrive and be erected. It was whilst travelling to Essexvale that Selous met his old friend, Mr. Helm, the missionary, who by his long residence amongst the Matabele was thoroughly conversant with native views. Mr. Helm said that on the whole the natives had accepted the new regime, but that they were highly incensed at the confiscation of their cattle by the Chartered Company. The natives at first were told that after all the cattle had been branded with the Company's mark and handed back to the natives, only the king's cattle would be confiscated. "This promise," says Selous, "was made under the belief that nearly all the cattle in Matabeleland had belonged to the king and that the private owners had been but few in number." This was a great mistake, for nearly every chief induna and men of any position had possessed large herds of their own.

At Bulawayo Selous found a ruined kraal, since it had been burnt and deserted by the Matabele after their defeat in 1893. The site of the new town had been marked out by the settlers, who had camped close by, and a general air of hope and prosperity hung over the scene of the new British town that was shortly to arise from the ashes of the past. No difficulties with the natives were apprehended, and farms and town-sites were at a high value. No one, in fact, dreamed that in a few months the whole country would be overwhelmed in the calamity of the rinderpest—a cattle disease that swept from Abyssinia to the Cape and killed in its course nearly the whole stock of cattle, as well as many fine species of game, such as buffalo, eland, koodoo, etc. Added to this the Matabele again rose, burnt the farms, and in many cases murdered all the new settlers and carried destruction throughout the whole country north of the Limpopo. To add to these horrors a bad drought and an unusual plague of locusts rendered farming and transport practically impossible.

There were some 70,000 cattle at this time in the hands of the natives, and a final settlement was made by which the Chartered Company retained two-fifths, giving the remaining three-fifths to the natives, a settlement by which for the time being the natives appeared satisfied.