Various ingredients are used to effect case-hardening. One process is as follows: 20 lbs. of scrap leather and 15 lbs. of hoofs (cut into pieces of about an inch square), 4 lbs. of salt, and one gallon of urine are prepared, and a wrought iron box with a lid capable of being fastened on is obtained. The fastenings must be capable of ready unfastening when hot. A layer of leather and pieces of hoofs about 11⁄2 inches thick is first laid in the box, then a layer of salt, and then a layer of work. Leather and hoof are then packed closely around the work and above it for a thickness of about an inch, and a second layer of work added, and so on, the last layer being of leather, &c., completely filling the box; the urine is then added, and the box well sealed with clay.
The box is placed in a furnace and kept at a red heat for about fourteen hours, and is then taken to a deep tank, and the work quickly immersed, so as not to be exposed to the air after the box is opened.
If the pieces are of solid proportions, so as not to be liable to bend or warp in the cooling, the contents of the box are simply dumped into the tank, the water being allowed to flow freely in the tank to keep up a circulation and cool the work quickly; some work, however, requires careful dipping to prevent it from warping. Thus a link or a double-eye would be dipped endwise, a plate edgewise; but all pieces should be immersed as quickly as possible after the box is opened.
Sheehan’s patent process for box case-hardening, which is considered a very good one, is thus described by the inventor:
DIRECTIONS TO MAKE AND USE SHEEHAN’S PATENT PROCESS FOR STEELIFYING IRON.
No. 1 is common salt.
No. 2 is sal soda.
No. 3 is charcoal pulverized.
No. 4 is black oxide of manganese.
No. 5 is common black rosin.