The Sulphur obtained, either by distillation or by simple fusion, is not always pure.
When it is obtained by distillation, if the matters from which you extract it contain moreover some other minerals of nearly the same volatility, such, for instance, as Arsenic, or Mercury, these minerals will come over with it. This is easily perceived: for pure sublimed Sulphur is always of a beautiful yellow, inclining to a lemon colour. If it look red, or have a reddish cast, it is a sign that some Arsenic hath risen along with it.
Mercury sublimed with Sulphur likewise gives it a red colour; but Sulphur is very seldom adulterated with this metallic substance: for Arsenic is frequently found combined with the Pyrites, and other sulphureous minerals; whereas, on the contrary, we very rarely meet with any Mercury in them.
But if Mercury should happen to rise with the Sulphur in distillation, it may be discovered by examining the sublimate; which, in that case, will have the properties of Cinabar: on being broken its inside will appear to consist of needles adhering laterally to each other; its weight will be very considerable; and, lastly, the great heat of the place where it is collected will furnish another mark to know it by; for, as Cinabar is less volatile than Arsenic or Sulphur, it fastens on places too hot for either Sulphur or Arsenic to bear.
Sulphur may also be adulterated with such fixed matters, either metallic or earthy, as it may have carried up along with it in the distillation, or as may have been sublimed by the Arsenic, which has a still greater power than Sulphur to volatilize fixed bodies.
If you desire to free the Sulphur from most of these heterogeneous matters, it must be put into an earthen cucurbit, and set in a sand-bath. To the cucurbit must be fitted one or more aludels, and such a degree of heat applied as shall but just melt the Sulphur; which is much less than that necessary to separate the Sulphur from its matrix. As soon as the Sulphur is melted it will sublime in lemon-coloured flowers, that will stick to the insides of the aludels.
When nothing more appears to rise with this degree of heat, the vessels must be suffered to cool. At the bottom of the cucurbit will be found a sulphureous mass, containing the greatest part of the adventitious matters that were mixed with the Sulphur, and more or less red or dark-coloured, according to the nature of those matters.
When we come to treat of Arsenic and Mercury, we shall give the methods of separating Sulphur entirely from those metallic substances.