In [Table 8] are given a series of corrections making it possible to use this method at any temperature between 50 and 80° Fahrenheit. The more closely the readings are taken to 68° F. the more accurate the results. Moreover, when it is attempted to strain the insoluble solids from hot pulp or cyclone juice, considerable evaporation occurs, causing concentration of the product and producing an error in the results. When hot pulp is handled, therefore, it must be strained as quickly as possible, and more accurate results may be obtained if the pulp is cooled quickly before straining. This may be done by placing in a large can and stirring vigorously while the can stands in ice water, or shaking under water in a large flask.
There are several forms of hydrometer which may be used for determining the specific gravity of the filtrate. The ordinary specific gravity hydrometer is the most logical form to use, since it gives the specific gravity directly. Unfortunately, specific gravity hydrometers with the particular marking required for this work are not a stock article, and would, therefore, have to be made to order. For this reason they would be difficult to obtain and not easily replaced if broken.
The Brix hydrometer appears to solve the difficulty. This hydrometer has no direct relation to specific gravity, but Brix readings can, of course, be converted to the specific gravity readings by a table arranged in parallel columns. [Table 9] gives the specific gravity of tomato pulp and the corresponding Brix reading of the filtrate. The Brix hydrometer gives directly the per cent of sugar in a solution of cane sugar, one degree Brix being equivalent to one per cent sugar at the temperature for which the hydrometer was calibrated. This fact and the ordinary purpose for which the instrument is manufactured are of no interest to us in this connection, however. The Brix hydrometer of the range desired for the examination of cyclone juice and pulp is a stock article and can be secured readily.
The instrument can be used with the same accuracy as the specific gravity hydrometer, and the results obtained by it, after correcting for temperature by [Table 8], are converted into terms of specific gravity by means of [Table 9]. The determination of the specific gravity of pulp by means of the hydrometer reading of the filtrate obtained from the pulp has several advantages over the ordinary method of weighing a measured quantity of the pulp. When applied to pulp manufactured from whole tomatoes, the method is reasonably accurate. It is also very rapid and the equipment required is inexpensive. This method is especially applicable to the examination of pulp manufactured from whole tomatoes. It is less applicable to trimming stock pulp, although even with that product the method will be of value, especially for the examination of cyclone juice for the purpose of controlling concentration. With pulp manufactured from trimming stock, the relation of the specific gravity of the pulp to the specific gravity of the filtrate obtained from it will vary according to the nature of the raw material used and also according to the method of manufacture. It seems probable, therefore, that after a manufacturer has determined this relation as applied to his own product, he may be able to use this method with reasonable accuracy even in connection with trimming stock pulp.
The method is adapted especially to the examination of cold pulp or cyclone juice.
- 1 Brix hydrometer, graduated at 20.0° C., with a range of 1–10°, graduated in 1/10°.
- 1 Cylinder of heavy glass, lipped, height 12 inches, diameter 2 inches.
- 1 Chemical thermometer, graduated in Fahrenheit system up to 212° F.
Since this apparatus is likely to be broken, it is well for each plant that contemplates using the method to equip itself with at least two of each item mentioned above.
The Brix hydrometer mentioned above is suggested because it is a stock article handled by all dealers in chemical apparatus and can be secured quickly. It has the disadvantage that it is relatively large, and in order to use it the filtrate must be prepared in much larger quantity than would be required by a smaller hydrometer. By placing orders well in advance with dealers in chemical apparatus special hydrometers may be made with a bulb about one-half inch in diameter and with a total length of five or six inches. Such hydrometers could be used with a cylinder as small as one inch in diameter. They would require much less liquor than is necessary for the Brix hydrometer and therefore would enable the analyst to obtain results much more quickly. In securing such hydrometers it would be well to order several at a time, since it would require several weeks to replace any that may be broken.
The details of the method are as follows:
Place a piece of cotton cloth of about the texture of ordinary glass toweling over a clean, dry container 10 or 12 inches in diameter or over a No. 10 can. Pour on the cloth a suitable amount of the pulp or cyclone juice to be examined, pick the cloth up by the corners and squeeze gently to separate the greater part of the insoluble solids. The strained liquid left in the vessel will be more or less turbid, according to the pressure exerted in squeezing. The amount of insoluble material producing this turbidity, however, is not usually sufficient to interfere with the examination of the product by means of a hydrometer. If, however, it is necessary to exert considerable pressure to get the amount of filtrate desired and the turbidity is therefore considerable it will be necessary to pass the liquor through a second filter, which, of course, may be done quickly.