Subsidence Method.—When a small amount of soil is stirred up in water, and is afterward allowed to stand for some time, the different grain-sizes will settle consecutively in accordance with their sizes (or weights); the smallest ones settling latest, and the clay only remaining suspended, as stated above. So long, however, as any considerable amount remains suspended in the water, the latter is not only denser but especially more viscid than if the clay were absent. In order therefore to obtain correct results by any method involving the use of water, it is necessary to remove the clay before proceeding to the separation of the granular sediments. This, as has been already stated, is approximately accomplished by allowing the soil, when diffused in water after proper disintegration, to settle for 24 hours from a column of water 200 mm. high, whereby all grain-sizes, of and above .01 mm. diameter are removed from the turbid liquid. This sedimentation is then repeated until after 24 hours the water becomes clear. The clay is then determined in the “clay water” by evaporation or precipitation; the granular sediments may then be successfully separated by sedimentation.
The U. S. Bureau of Soils uses for the separation of clay, instead of subsidence for 24 hours, the more expeditious process of centrifuging the turbid soil water in appropriate glass cylinders, by the aid of an electric motor; and thus in a relatively short time obtains “clay” in which the upper limit of size is one-half of that mentioned above, viz., .005 mm. But for the costliness of the appliances required, including the entire time of an operator, this method of separating the clay would undoubtedly be preferable to the elimination by subsidence; the more as a more minute grain-size for the clay group is thus secured.
Fig. 6.—
Schöne’s
Elutriator.
The separation of the clay having been accomplished, the various sizes of silt and sand may be separated by again suspending them in water; and interrupting the settling process at stated times, the grain-sizes corresponding to definite velocities in settling may be segregated and weighed. When this process of settling and decanting is carefully and repeatedly carried out, very good results are obtained.
Hydraulic Elutriation.—The sedimentation (or “beaker”) method, long practiced in the arts is, however, quite tedious, requiring the constant close attention of a skilled observer. The desired results may, in the writer’s judgment, be more conveniently obtained by the hydraulic method, whenever no very large volume of work of this kind is required to be done at once.
When instead of allowing the soil to settle in quiet water, the latter is used as an ascending current of regularly graded velocities, it is clear that the soil particles will be carried off by this current in exact conformity with their several sizes (or strictly speaking, volume-weights); and when maintained in such a current for a sufficient length of time, the entire quantity of the sediment corresponding to the prevailing velocity will be carried away. It is of course easy to ascertain to what grain-sizes certain velocities of the upward current (regulated by a stopcock with arm moving on a graduated scale) correspond, and to regulate accordingly the intervals between the different velocities to greater or less detail, as may be desired. A number of instruments have been devised for this purpose.
Schöne’s Elutriator is the one commonly used in Europe; in it the upward current ascends in a conical glass tube, ([see figure 6]) entering through a narrow, curved inlet tube, in which the soil sample is kept agitated by the current itself. The objection to this plan is twofold: first, the narrow, curved inlet-tube is readily clogged by the soil mass at the lower velocities, which are thereby changed, so that, unless a very small amount of soil only is employed, the whole mass is not kept properly stirred; second, the circulating currents brought about by the conical shape of the tube cause the sediment-particles to coalesce into complex, larger ones (floccules), which will then settle down and fail to pass over at the current-velocity corresponding to their individual component parts.
Fig. 7.—The Churn Elutriator (Hilgard’s)
for the physical analysis of soils.