Churn Elutriator with Cylindrical Tube.—The errors just alluded to are obviated by an arrangement devised by the writer, in which a rapidly revolving stirrer, placed at the base of a cylindrical tube in which the washing process is conducted and which eliminates counter-currents, continually disintegrates these compound particles, and thus enables the entire quantity of the sediment corresponding to the prevailing current-velocity to pass off with a comparatively slight expenditure of time on the part of the operator ([see figure 7]). A wire screen interposed between the churn and cylindrical glass tube prevents communication of the whirling motion to the column. As the apparatus works automatically, the analyst has only to observe from time to time whether or not the turbidity near the top of the tube has disappeared; and as the sediment accumulates at the bottom of the tall receiver bottle,[25] no harm is done if the attendant should neglect to change the velocity in time, except that water will run to waste.
The conical relay glass below the churn serves to retain the coarser grades of sediments which are not concerned in the velocities employed in the elutriator tube, and thus prevents injurious attrition. But these sediments can at any time be stirred up by the incoming current and brought into the washing tube if desired. In the same manner the passing-off of the finer sediments can be materially accelerated by running off rapidly about two-thirds of the turbid column of water every twenty minutes.
It should be fully understood that prior to attempting such separation, the “colloidal clay” must first be removed by the subsidence or centrifugal method, since otherwise much larger grain-sizes may be carried off at a given velocity.
Yoder’s Centrifugal Elutriator.—A very ingenious instrument which combines the elutriation and sedimentation processes into one, has been devised by P. A. Yoder, of the Utah Expt. Station. The elutriator bottle is placed in a centrifuge driven by an electric motor; it is closed by a glass stopper carrying a delivery tube to a short distance above the bottom of the elutriator bottle, as well as an outflow tube ending at the base of the stopper; the latter also carries a funnel coinciding with the center of rotation. Into this funnel flows gradually the muddy water containing the soil in suspension; and the rate of its flow, together with the velocity of rotation, determines the size of the sediment-granules that will be deposited in the slack-water below the mouth of the delivery tube. The muddy soil-water is kept agitated in a funnel-shaped reservoir by air-bubbles from a constant-pressure chamber.
While the principle of this instrument is good, it is quite complicated and the results obtainable from it in practice have not as yet been made public. The inventor claims that an analysis may by its means be completed in less than three hours.
In all hydraulic elutriators a provision for constant pressure in the reservoir supplying the current of water is needed; although in Schöne’s and some other instruments a gradually decreasing pressure in a plain reservoir is employed. A large glass bottle or carboy fitted with the proper tubes so as to constitute a Mariotte’s bottle (in which the air enters near the bottom of the vessel), is a very convenient arrangement.
Number of Sediments.—The number of grain-sizes or sediments into which the soil mass is to be segregated is of course entirely within the option of the operator. Experience has shown that it is unnecessary to discriminate very closely between the several sizes of the coarser portion of the sand, such as those lying between one-fourth and one-half of a millimeter. But below this point, and especially between one-tenth of a millimeter and the clay, a proper discrimination becomes very important. The series first devised by the writer in 1872 is based upon a consecutive doubling of the velocities of the current from a quarter of a millimeter per second to thirty-two millimeters per second; the sediment of sixty-four millimeter-velocity corresponding to a diameter of one-half of a millimeter, will remain in the elutriator. Above this, as before remarked, the sieve (especially when aided by a jet of water) effects a satisfactory segregation.
The table below shows the elements of these series both as regards current-velocities and maximum quartz-grain diameters carried off by each. In a great many cases, however, it is altogether unnecessary to go into such detail, and a subdivision into six or seven divisions is quite sufficient. Such a subdivision, based upon the doubling of grain-sizes instead of current-velocities, has been adopted by Prof. Milton Whitney, of the U. S. Department of Agriculture, and others.
TABLE OF DIAMETERS AND HYDRAULIC
VALUES OF SEDIMENTS.
| Designation of materials. | Velocity per second, or hydraulic value. | Maximum diameter of quartz grains. |
|---|---|---|
| Mm. | Mm. | |
| Grit | (?) | 1-3 |
| Sand | (?) | .5-1 |
| 32-64 | .50 | |
| 16-32 | .30 | |
| 8-16 | .16 | |
| 4-8 | .12 | |
| Silt | 2-4 | .072 |
| 1.0-2 | .047 | |
| .5-1 | .036 | |
| .25-0.5 | .025 | |
| 0.25 | .016 | |
| 0.25 | .010 | |
| Clay | 0.0023 |