It is best to separate the water and oil in a regular separatory funnel, or in a simple apparatus illustrated in Fig. 4. It is made by cutting the bottom from a tall flask, and fitting into the neck by means of a cork a glass tube having a diameter of one-fourth to one-half inch. A rubber tube with stop-cock is fastened to the glass tube. By careful opening of the stop-cock, the watery fluid can be drained off to the last drop.
To the perfumer this method is of little importance, since it is applicable only to a few substances which, moreover, give cheap odors. Still, the possession of a hydraulic press is advisable to every manufacturer who works on a large scale, as it is useful also in the preparation of several fixed oils frequently employed in perfumery, for instance, oils of almonds, nuts, etc.
Fig. 5.
Fig. 6.
Fixed oils are best extracted in so-called drop presses, the material having first been comminuted between rollers. These are arranged as shown in section in Fig. 5, and in ground plan in Fig. 6. The apparatus consists of two smooth or slightly grooved iron cylinders A and B, respectively four feet and one foot in diameter, which can be approximated or separated by means of set screws. The material is placed into the trough F containing a feeding roller moved by the belt P. The scrapers FF, pressed against the cylinders by means of weighted levers, free the rollers from adhering pieces.
The drop presses Figs. 7 and 8 consist of a hydraulic press with cylinders A and piston B; the troughs E are movable by means of rings between two vertical columns and every trough has a circular gutter d for the reception of the expressed oil. The iron pots G have double walls, the inner of which has a series of openings at its upper part; these pots are filled with the bruised material to be pressed and after this has been covered with a plate of horse-hair tissue are set in the press.
Fig. 7. Fig. 8.