Formula for Caffein, Showing Its Relation to the Purin Group

Gorter states that caffein exists in coffee in combination with chlorogenic acid as a potassium chlorogenate, C32H36O19, K2(C8H10O2N4)2·2H2O, which he isolated in colorless prisms. This compound is water-soluble, but caffein can not be extracted from the crystals with anhydrous solvents. To this behavior can probably be attributed the difficulty experienced in extracting caffein from coffee with dry organic solvents. However, the fact that a small percentage can be extracted from the green bean in this manner indicates that some of the caffein content exists therein in a free state. This acid compound of caffein will be largely decomposed during the process of torrefaction, so that in roasted coffee a larger percentage will be present in the free state. Microscopical examination of the roasted bean lends verisimilitude to this contention.

Planter's Bungalow with Coffee Trees in Flower, Mysore

Coolies Bagging Coffee on the Drying Grounds
COFFEE SCENES IN BRITISH INDIA

Table II—Coffee Analyses
Santos
Green
Santos
Roasted
Padang
Green
Padang
Roasted
Guatemala
Green
Guatemala
Roasted
Mocha
Green
Mocha
Roasted
Moisture April 20th8.753.758.782.729.593.409.063.36
Moisture September 20th8.126.458.056.038.686.928.157.10
Ash4.414.494.234.703.934.484.204.43
Oil12.9613.7612.2813.3312.4213.0714.0414.18
Caffein1.871.811.561.471.261.221.311.28
Caffein, dry basis2.03——1.69——1.39——1.44——
Crude fiber20.7014.7521.9214.9522.2315.2322.4615.41
Protein9.5012.9312.6214.7510.4311.698.569.57
Protein, dry basis10.41——13.68——11.53——9.41——
Water extract31.1130.3030.8330.2131.0430.4731.2730.44
Specific gravity, 10 percent extract 1.0109 1.0101 1.0107 1.0104 1.0105 1.0404 1.0108 1.0108
Bushelweight47.028.245.227.852.227.248.830.2
1,000 kernel weight103.60120.20167.30151.35189.20165.80119.52100.00
1,000 kernel weight, dry basis119.1115.7154.1147.2171.0160.1108.696.6
Dextrose——0.72——0.81——0.54——0.46
Caffetannic acid.5817.4415.3716.9316.2717.1315.6116.89
Acidity by titration apparent1.502.081.472.001.392.131.111.87