GERMANY.
Calcic salt elimination from beet juices is a problem not yet satisfactorily solved. Since the early history of beet sugar making, it has been noticed that calcic salts render graining in the pan most tedious; hence repeated efforts to reduce to a minimum percentage the use of lime during defecation. In all cases it is essential to get rid of inverted sugar. The difficulty from excess of lime is overcome by adding it now and then during carbonatation; but other means are found desirable; and phosphoric acid, magnesia, soda, etc., have been used with success. Recent observations relating to the action of soda upon calcic sulphates, calcic glucates, etc., are most important. Certain citrates have a retarding influence upon calcic sulphates.
An alarm contrivance to announce the passage of juices into condensing pipes has rendered considerable service in beet sugar factories.
A process for refining sugar in the factory, at less cost than it is possible to make raw sugar by existing processes, deserves notice. Sugars by this new method test 99.8, and sirups from the same have a purity coefficient of 70. Weight of dry crystals obtained is said to represent 66 per cent. of masse cuite used. The additional cost of the process is $30 to $40 per centrifugal. Concentrated juice or sirup may be used as cleare in centrifugals; this sirup should have a density of 1.325 (36° B.) at 113° to 122° F., so as not to redissolve the sugar. Sirup should not be used until all adhering sirup of masse cuite has been swung out. The sirup, after passing through centrifugals, may be sent to second carbonatation tanks and mixed with juices being treated.
The larva of an insect, known as sylpha, has attacked beet fields in several parts of Saxony. The effect upon the root is a decrease in foliage, followed by late development of the beet, with corresponding reduction in sugar percentage. Chickens may render excellent service, as they eat these worms with considerable relish. A solution of Schweinfurt green has been used with some success; its cost is $2.50 per acre. None of the chemical remains on the leaves after a rain (?) White worms have done some damage; they should be collected from the fields during plowing. When they become beetles in the spring, they may be destroyed by a solution of sulphide of carbon; $0.20 worth of this chemical is sufficient to kill 10,000 of them. These beetles contain 50 per cent of fatty and nitric elements; when pulverized they may be used as good for pigs and chickens. If the ground mass of beetles is sprinkled with sulphuric acid and a reasonable amount of lime and earth be added, the combination forms an excellent fertilizer for certain crops. A disease that blackens young beet leaves is found to be due to a microscopic insect. If the beet seed be saturated in a phenic solution before planting, the difficulty may be overcome.
We are soon to have a new method for selecting mothers for seed production. Details of the same are not yet public. It is claimed that it will be possible to grow seed that will yield beets of a given quality determined in advance, a problem which has hitherto been thought impossible.
It will surprise many of our readers to learn that if "tops" or even half beets are planted, they will give seed, the quality of which is about same; showing that as soon as seed stalks commence to appear, the role of the root proper is of secondary consideration, as it serves simply as a medium between the beet and soil(?)
Sprayed water may be used with considerable success in washing sugar in centrifugals; it is claimed that this new process offers many advantages over either steam, water, or use of cleare. White sugar to be washed is thoroughly mixed with a sugar sirup supersaturated. The whole is run into centrifugals. The sirup swung from the same is used in next and following operations; when it becomes too thick it is sent to the vacuum pan to be regrained. The operation of washing lasts less than two minutes; three quarts of water are necessary for 200 lb. sugar. The water spray at a pressure of 5 to 10 atmospheres is produced by a very simple appliance.
Total weight of refuse cossettes obtained during last campaign was 4,000,000 tons, about 700,000 tons of which were sold for $1,000,000; if what remains is dried, it would be worth $5,000,000.
Several sodic-baryta methods have been recently invented. Of these we will mention one where 1/4000 to 1/2000 part of calcined soda is added to the beet slices in diffusors. The juice when drawn from the battery is heated to 154° F., and defecated with hydrate of baryta and milk of lime. Nearly all foreign substances are thus eliminated. Carbonatation then follows.
Government taxation upon the sugar industry is destined within a few years to be withdrawn. The new law recently put into operation no longer taxes beets worked at factory, but the sugar manufactured. The rate of taxation is about 2 cents per pound on all sugar made.
Recent data from northeast Germany give the work during campaign 1890-91 of 54 associated beet sugar factories. They used 2,130,000 tons beets, obtained from 142,602 acres of land, average yield 12 tons. The total sugar amounted to 251,000 tons, of which 241,000 were from beets and 10,000 tons from molasses worked by special processes. The polarization of beet juices averaged 13.09; masse cuite, 14.31; extraction of sugar of all grades, 11.79. It required 848 lb. beets to produce 100 lb. sugar.
In every center where beet sugar is made there exists some local society; each year members from these societies meet to exchange views upon the sugar situation of the empire.
Of late, there has been a general complaint respecting quality of sugar sold on the Magdeburg market. At one time the sugars averaged more organic substances than ash; now there is more ash than organic substances. Such sugars are most difficult to work, and cause much loss of time in centrifugals.
The most desirable temperature for diffusion batteries is not yet definitely settled. Some manufacturers recommend 82° to 86° F. On the other hand, satisfactory results have been obtained at 145° F., followed by cold water in the diffusors.
The use of hydrofluoric acid, even in small quantities to prevent fermentation, should not be allowed.
It is proposed to use hydrogen dioxide for saccharine juice purification. The alkalinity of juice is reduced to 0.07 by a judicious use of lime. Precaution must be taken to keep the temperature at 87° F. After a preliminary filtration about 4 per cent. hydrogen dioxide is added. The whole is then heated to the boiling point, after which ½ to 1 per cent. lime is added. When alkalinity of filtrate is 0.03 phosphoric acid and magnesia are added, in quantities representing 0.03 per cent. of sugar in juice for magnesia, and 0.6 per cent. for the phosphoric acid. In working beet juices hydrogen dioxide may be used in the diffusor or during any phase of the sugar manufacturing process, even upon sugars in centrifugals. In all cases the results obtained are said to be most satisfactory.
A method to crystallize the sugar contained in the mother liquor of a masse cuite consists in mixing during 24 hours the hot product, direct from the pan, with low grade molasses. Gradual cooling follows. The crystals of masse cuite effect a crystallization of the otherwise inactive product contained in the molasses. The separation of crystals from adhering molasses is done in a special washing appliance arranged in battery form.
It has been frequently asked if the existing and accepted formula for determining in advance the amount of refined sugar that may be extracted from either beets, masse cuite or raw sugar, is to be considered exact, without special allowance being made for raffinose. An intelligent discussion upon the subject shows that the sugar in question, whether present or not, in no way influences the formula under consideration.