“The writer cannot recall all the doubts, fears, optimism, and enthusiasm felt in turn by different members of the organization during the fabrication of those first 20,000 masks. We were performing an important task for the War Department. Night became day. Dewey, Lewis, Henderson, Gibbs, and others stepped from one train to another, and we used the telephone between Washington and St. Louis or Boston as freely as we used the local Washington telephone.
“We thought we could improve on the English box respirator on various points. We made the canister larger, and have been glad ever since that we did. We thought the English mouthpiece was too flexible and too small, and made ours stiff and larger, and were sorry we made the change. We tested the fillings against chlorine, phosgene, prussic acid, etc., and had a canister that was all that was desired for absorbing these gases. But, alas, we did not know that chloropicrin was destined to be one of the most important war gases used by the various belligerents. Further, it was not fully appreciated that the rubberized cloth used in making the facepiece had to be highly impermeable against gases, that hardness as much as anything else was desired in the make-up of the soda-lime granules in order to withstand rough jolting so that the fines would not clog the canister, and raise the resistance to breathing to a prohibitive figure. Neither was it appreciated at that time by any of the allies, that the gas mask really should be a be a fighting instrument, one that men could work hard in, run in, and wear for hours, without too serious discomfort.
“The first 20,000 masks sent over to England were completed by the Research Division in record time. As compared with the French masks, they were far superior, giving greater protection against chlorine, phosgene, superpalite, prussic acid, xylyl bromide, etc. The French mask was of the cloth type, conforming to the face, and consisting of twenty layers of cheesecloth impregnated with sodium phenate and hexamethylenetetramine. Chloropicrin went through this like a shot. Just before the masks were sent abroad, we received disturbing rumors of the contemplated use of large quantities of chloropicrin. The French, apparently, had no intention of changing the design of their mask, and did not do so for months to come. We therefore released the masks, they were sent abroad, and an anxious research group on this side of the water waited expectantly for the verdict. It came. A brief cablegram told us what our English cousins thought of us. It was a subject they had been wrestling with for two years and a half. They had had battlefield experience; they had gone through the grief of developing poor masks into better ones, knew the story better than we did, and after a thorough test ‘hammered’ the American design unmercifully.
“This experience put the Research Division on its mettle. Our first attempt had given us the necessary preliminary experience; cablegrams and reports traveled back and forth; an expert or two eventually came to this country from England in response to previous appeals for assistance, and we turned with adequate information to the development of a real mask.”
The story of mustard gas is given later. It probably occupied more time and thought on the part of the Research Division, as well as that of Edgewood Arsenal and the Development Division, than any other gas.
Diphenylchloroarsine led to the preparation of a series of arsenic compounds, some more easily prepared and more or less effective.
Cyanogen chloride and cyanogen bromide, reported by the Italians as having been used by the Germans, were extensively studied.
The Inorganic Section was early interested in special incendiary materials which were developed for bombs, shells, darts and grenades, and which were later taken over by the Pyrotechnic Section, and finally adopted by the Ordnance Department.
In discussing the work one can very well start with the Offense Section. This Section had two aims in view always, to develop methods of making the gases used by the Germans more economically than they were making them, and to develop better gases if possible. When we entered the war, chlorine, phosgene and chloropicrin were the lethal gases used, while bromoacetone and xylyl bromide were the lachrymators. It was not a difficult matter to prepare these. But the introduction of mustard gas in the summer of 1917 and of diphenylchloroarsine in the autumn of the same year, not only made our chemists ponder over a manufacturing method, but also so revised our notions of warfare that the possibility of using other substances created the need for extensive research. The development of bromobenzylcyanide by the French likewise opened a new field among lachrymatory substances.
Colored rockets and smokes were developed for the Navy and Army. The smoke box was also studied but the work was taken over by the Pyrotechnic Section.